摘要：【中文】一种丁香酚完全抗原的合成方法，本发明涉及化学物合成技术领域；丁香酚羧基化半抗原的制备；称取丁香酚羧基化半抗原，溶于1mL PBS缓冲液中；称取12mg载体蛋白溶于1mL PBS缓冲液中，得到载体蛋白溶液，然后将半抗原溶液逐滴加入到载体蛋白溶液，得到半抗原和载体蛋白混合溶液；将5mg EDC溶于0.5mL PBS缓冲液中，得到EDC溶液，然后将EDC溶液边搅拌边逐滴加入上一步得到的半抗原和载体蛋白混合溶液中，继续冰浴15min，室温下振荡反应1h，反应结束后，用PBS透析；对丁香酚完全抗原的鉴定。制备的丁香酚完全抗原弥补了丁香酚免疫学检测方法技术领域的空白，为丁香酚酶联免疫检测方法的进一步发展奠定了基础。 【EN】The invention discloses a synthetic method of a eugenol complete antigen, and relates to the technical field of chemical synthesis; preparing eugenol carboxylation hapten; weighing eugenol carboxylated hapten, and dissolving the eugenol carboxylated hapten in 1mL of PBS buffer solution; weighing 12mg of carrier protein, dissolving the carrier protein in 1mL of PBS buffer solution to obtain a carrier protein solution, and then dropwise adding the hapten solution into the carrier protein solution to obtain a mixed solution of the hapten and the carrier protein; dissolving 5mg of EDC in 0.5mL of PBS buffer solution to obtain EDC solution, then dropwise adding the EDC solution into the mixed solution of the hapten and the carrier protein obtained in the previous step while stirring, continuously carrying out ice bath for 15min, carrying out oscillation reaction at room temperature for 1h, and dialyzing with PBS after the reaction is finished; and (3) identifying a eugenol complete antigen. The prepared eugenol complete antigen makes up the blank of the technical field of eugenol immunological detection methods, and lays a foundation for the further development of eugenol enzyme-linked immunosorbent assay methods.

摘要：【中文】本发明涉及锂离子电池领域，公开了一种电解液，包括高温型有机溶剂、正负极保护添加剂及电解质锂盐；其中，高温型有机溶剂包括以下重量份数的各组分：碳酸乙烯酯5～30份、碳酸丙烯酯5～30份、碳酸二乙酯5～30份、丙酸丙酯5～50份及氟苯1～10份；正负极保护添加剂包括以下重量份数的各组分：硫酸乙烯酯0.2～5份、氟代碳酸乙烯酯0.2～5份、二氟碳酸乙烯酯0.2～5份、二腈类有机物0.2～5份、二氟磷酸锂0.2～3份、双乙二醇双丙腈醚0.2～5份、氟磺酰亚胺锂0.2～3份、1‑丙基磷酸酐0.1～2份、1,1,2,2‑四氟乙基‑2,2,3,3‑四氟丙基醚0.5～20份、二氟草酸硼酸锂0.1～2份及甲烷二磺酸亚甲酯0.1～1份。本电解液耐高温性能优异，能够使具有高能量密度的锂离子电池在70℃以上温度下也能正常工作，且能够保持较佳的续航能力。 【EN】The invention relates to the field of lithium ion batteries, and discloses an electrolyte, which comprises a high-temperature organic solvent, an anode and cathode protection additive and electrolyte lithium salt; the high-temperature organic solvent comprises the following components in parts by weight: 5-30 parts of ethylene carbonate, 5-30 parts of propylene carbonate, 5-30 parts of diethyl carbonate, 5-50 parts of propyl propionate and 1-10 parts of fluorobenzene; the anode and cathode protection additive comprises the following components in parts by weight: 0.2-5 parts of vinyl sulfate, 0.2-5 parts of fluoroethylene carbonate, 0.2-5 parts of difluoroethylene carbonate, 0.2-5 parts of dinitrile organic matter, 0.2-3 parts of lithium difluorophosphate, 0.2-5 parts of diethylene glycol dipropionitrile ether, 0.2-3 parts of lithium fluorosulfonylimide, 0.1-2 parts of 1-propylphosphoric anhydride, 0.5-20 parts of 1,1,2, 2-tetrafluoroethyl-2, 2,3, 3-tetrafluoropropyl ether, 0.1-2 parts of lithium difluorooxalato borate and 0.1-1 part of methylene methanedisulfonate. The electrolyte has excellent high-temperature resistance, can ensure that the lithium ion battery with high energy density can normally work at the temperature of more than 70 ℃, and can keep better cruising ability.

摘要：【中文】本申请公开了一种纳米材料，所述纳米材料具有多孔卟啉金属有机骨架，所述纳米材料为椭圆球形纳米颗粒，所述纳米材料的孔径为1.0nm～5.0nm；所述纳米材料的比表面积为1000m²g^‑1～2300m²g^‑1。本申请提供的纳米材料具有对于Cu²⁺高度选择性和灵敏性，呈现了溶剂适应性，克服了天然卟啉酶例如HRP的缺点。 【EN】The application discloses a nano material, which is provided with a porous porphyrin metal organic framework, the nano material is oval spherical nano particles, and the aperture of the nano material is 1.0-5.0 nm; the specific surface area of the nano material is 1000m²g^‑1～2300m²g^‑1. The nano material provided by the application has the characteristics of being specific to Cu²⁺High selectivity and sensitivity, and solvent adaptability, and overcomes the disadvantages of natural porphyrases such as HRP.