摘要：【中文】本发明公开了一种二氟草酸硼酸锂的制备方法，包括如下步骤：S1、向草酸锂溶液中加入三氟化硼乙腈，进行反应得到反应液，然后加入反溶剂搅拌，过滤得到滤液A和滤饼B；S2、向滤液A中加入无水草酸、助剂，进行反应，过滤，取滤液析晶得到物质C，取物质C与滤饼B混匀，重结晶得到二氟草酸硼酸锂，其中，助剂为氯化铁、氯化钙、氯化铜中的至少一种。本发明工艺简单，易于操作，避免了环境污染和生产的危险性，原料来源可靠，制得的二氟草酸硼酸锂收率高，纯度好。 【EN】The invention discloses a preparation method of lithium difluoro (oxalato) borate, which comprises the following steps: s1, adding boron trifluoride acetonitrile into the lithium oxalate solution, reacting to obtain a reaction solution, adding an anti-solvent, stirring, and filtering to obtain a filtrate A and a filter cake B; s2, adding anhydrous oxalic acid and an auxiliary agent into the filtrate A, reacting, filtering, taking the filtrate for crystallization to obtain a substance C, uniformly mixing the substance C with the filter cake B, and recrystallizing to obtain the lithium difluoro oxalato borate, wherein the auxiliary agent is at least one of ferric chloride, calcium chloride and copper chloride. The method has the advantages of simple process, easy operation, avoidance of environmental pollution and production danger, reliable raw material source, high yield of the prepared lithium difluoro (oxalato) borate and good purity.

摘要：【中文】本发明公开了一种二氟双草酸磷酸锂的制备方法，包括如下步骤：S1、六氟磷酸锂溶液与草酸混匀，滴加硅氮烷，进行反应得到二氟双草酸磷酸锂、氨气和副产物氟硅氮烷；S2、副产物氟硅氮烷与氨气反应得到硅氮烷，作为S1中的原料循环使用。本发明通过溶剂法制备二氟双草酸磷酸锂，制备过程简单、副产物少且可回收利用、收率高，生产过程中没有废水产生，工艺路线绿色环保，所得二氟双草酸磷酸锂纯度高，适合工业化生产。 【EN】The invention discloses a preparation method of lithium difluorobis-oxalate phosphate, which comprises the following steps: s1, uniformly mixing the lithium hexafluorophosphate solution with oxalic acid, dropwise adding silazane, and reacting to obtain lithium difluorobis (oxalate) phosphate, ammonia gas and a byproduct, namely fluorosilazane; s2, reacting the byproduct fluorosilazane with ammonia gas to obtain silazane, and recycling the silazane as the raw material in S1. According to the invention, the lithium difluorobis (oxalate) phosphate is prepared by a solvent method, the preparation process is simple, the byproducts are few and can be recycled, the yield is high, no wastewater is generated in the production process, the process route is green and environment-friendly, and the obtained lithium difluorobis (oxalate) phosphate has high purity and is suitable for industrial production.

摘要：【中文】本发明公开了一种二草酸硼酸锂的制备方法，包括如下步骤：将草酸和碱性锂源加入非质子性溶剂中，搅拌回流反应，脱除非质子性溶剂和水，然后加入六甲基二硅氮烷、硼酸、季铵盐，进行反应，脱除副产物得到粗品，粗品提纯得到二草酸硼酸锂。本发明通过溶剂法制备二草酸硼酸锂，容易脱水和提纯，反应产物中含有极少量的水分，甚至不含水分，从而最大程度地降低了产物中水分的含量，有效解决水分对提纯的影响，简化了制备过程，提高了产物收率，所得二草酸硼酸锂纯度高，工艺简单，反应条件易于控制，更适合工业生产。 【EN】The invention discloses a preparation method of lithium oxalato borate, which comprises the following steps: adding oxalic acid and an alkaline lithium source into an aprotic solvent, stirring and carrying out reflux reaction to remove the aprotic solvent and water, then adding hexamethyldisilazane, boric acid and quaternary ammonium salt, carrying out reaction, removing byproducts to obtain a crude product, and purifying the crude product to obtain the lithium bis (oxalato) borate. The lithium bis (oxalato) borate is prepared by a solvent method, so that the lithium bis (oxalato) borate is easy to dehydrate and purify, and the reaction product contains very little moisture or even no moisture, so that the moisture content in the product is reduced to the maximum extent, the influence of the moisture on purification is effectively solved, the preparation process is simplified, the product yield is improved, the purity of the obtained lithium bis (oxalato) borate is high, the process is simple, the reaction condition is easy to control, and the method is more suitable for industrial production.

摘要：【中文】本发明公开了一种联产双氯磺酰亚胺酸和双氟磺酰亚胺锂的制备方法，包括如下步骤：S1、将硫酰氯加入第一溶剂中，再滴加八甲基环四硅氮烷，进行反应，纯化得到双氯磺酰亚胺酸；S2、取双氯磺酰亚胺酸、无水氢氟酸在催化剂作用下反应得到双氟磺酰亚胺酸；S3、取双氟磺酰亚胺酸、氟化锂在第二溶剂中进行反应，纯化得到双氟磺酰亚胺锂。本发明选用适宜的原料并配合溶剂法联产制备双氯磺酰亚胺酸和双氟磺酰亚胺锂，制备过程简单、副产物少且可回收利用，收率高，生产过程中没有水参与，所得双氯磺酰亚胺酸和双氟磺酰亚胺锂纯度高，无废水产生，工艺路线绿色环保，适合工业化生产。 【EN】The invention discloses a preparation method of coproduced dichlorosulfonyl imide acid and lithium difluorosulfonyl imide, which comprises the following steps: s1, adding sulfuryl chloride into the first solvent, dropwise adding octamethylcyclotetrasilazane, reacting, and purifying to obtain bischlorosulfonimidyl acid; s2, reacting the dichlorosulfonimide acid and anhydrous hydrofluoric acid under the action of a catalyst to obtain the difluorosulfonimide acid; s3, reacting the bis-fluorosulfonyl imide acid and lithium fluoride in a second solvent, and purifying to obtain the bis-fluorosulfonyl imide lithium. The method selects appropriate raw materials and is matched with a solvent method to coproduce and prepare the bis-chlorosulfonyl imide acid and the bis-fluorosulfonyl imide lithium, the preparation process is simple, the byproducts are few and can be recycled, the yield is high, no water is involved in the production process, the obtained bis-chlorosulfonyl imide acid and the bis-fluorosulfonyl imide lithium have high purity, no waste water is generated, the process route is green and environment-friendly, and the method is suitable for industrial production.

摘要：【中文】本发明公开了一种二氟草酸硼酸锂的制备方法，包括如下步骤：S1、向氟化锂悬浮溶液中加入三氟化硼碳酸二甲酯，进行反应得到反应液；S2、向反应液中依次加入无水草酸、助剂，继续反应，过滤，取滤液析晶，重结晶得到二氟草酸硼酸锂，其中，助剂为氯化铝、氯化铁、氯化钙、氯化铜中的至少一种。本发明通过选用适宜的助剂并配合溶剂法制备二氟草酸硼酸锂，容易提纯，简化了制备过程，提高了产物收率，有效降低了生产成本，生产过程中没有废水产生，工艺路线绿色环保，所得二氟草酸硼酸锂纯度高，适合工业化生产。 【EN】The invention discloses a preparation method of lithium difluoro (oxalato) borate, which comprises the following steps: s1, adding boron trifluoride dimethyl carbonate into the lithium fluoride suspension solution for reaction to obtain reaction liquid; and S2, sequentially adding anhydrous oxalic acid and an auxiliary agent into the reaction solution, continuing to react, filtering, taking the filtrate for crystallization, and recrystallizing to obtain the lithium difluoro-oxalato-borate, wherein the auxiliary agent is at least one of aluminum chloride, ferric chloride, calcium chloride and copper chloride. According to the invention, the lithium difluoro oxalate borate is prepared by selecting a proper auxiliary agent and matching with a solvent method, so that the purification is easy, the preparation process is simplified, the product yield is improved, the production cost is effectively reduced, no wastewater is generated in the production process, the process route is green and environment-friendly, and the obtained lithium difluoro oxalate borate has high purity and is suitable for industrial production.

摘要：【中文】本申请是关于一种化合物的性质分析方法、装置、设备及存储介质，涉及机器学习技术领域。该方法包括：根据化合物的分子结构获取该化合物的特征向量，该特征向量包括各个节点的节点向量和各条边的边向量；通过特征图提取模型分支对该特征向量进行处理获得图表示向量，通过分类模型分支对该图表示向量进行处理，获得该分类模型分支输出的该化合物的性质。上述方案可以结合化合物的特有分子结构组织化合物的特征向量，从化合物的特征向量中提取出能够准确表示化合物特征的图表示向量，从提高后续分类模型分支得到的分类性质的准确性。 【EN】The application relates to a method, a device, equipment and a storage medium for analyzing the properties of a compound, and relates to the technical field of machine learning. The method comprises the following steps: obtaining a characteristic vector of the compound according to the molecular structure of the compound, wherein the characteristic vector comprises a node vector of each node and an edge vector of each edge; and processing the characteristic vector through a characteristic diagram extraction model branch to obtain a diagram representation vector, and processing the diagram representation vector through a classification model branch to obtain the property of the compound output by the classification model branch. According to the scheme, the characteristic vectors of the compound can be organized by combining the specific molecular structure of the compound, the graph representation vector capable of accurately representing the compound characteristics is extracted from the characteristic vectors of the compound, and the accuracy of classification properties obtained by subsequent classification model branches is improved.

摘要：【中文】一种基于alpha稳定分布随机过程偏斜度参数的隐蔽通信方法，以有偏斜的alpha稳定分布随机序列作为载波，合法用户传输的隐蔽比特来调制前后半个比特周期载波序列的偏斜度极性，使之绝对值相同但极性相反，因此整个比特周期的隐蔽信号呈现出对称alpha稳定分布的特点；这种方法发射的隐蔽信号，与许多无线通信网络中存在的对称alpha稳定分布干扰非常相似，从而使得窃听者不易察觉到隐蔽通信的存在。本发明给出了计算量非常小的偏斜度的估计公式，以及推导出了相应的概率密度函数，得到了误比特率公式，指出了误比特率与特征指数、偏斜度、和样本数之间的关系。本发明实现容易、对设备计算性能要求不高的，隐蔽性较好。 【EN】A hidden communication method based on skew parameters in an alpha stable distribution random process is characterized in that a skewed alpha stable distribution random sequence is used as a carrier, and hidden bits transmitted by legal users modulate the skew polarity of the carrier sequence in the front half bit period and the back half bit period to make the absolute values of the carrier sequences identical but the polarities opposite, so that hidden signals in the whole bit period have the characteristic of symmetrical alpha stable distribution; the covert signal transmitted by this method is very similar to the symmetric alpha-stationary distributed interference present in many wireless communication networks, so that the presence of covert communication is not easily perceived by an eavesdropper. The invention provides an estimation formula of skewness with very small calculation amount and deduces a corresponding probability density function to obtain a bit error rate formula, and indicates the relationship between the bit error rate and the characteristic index, the skewness and the sample number. The invention has the advantages of easy realization, low requirement on the computing performance of equipment and better concealment.

摘要：【中文】本发明公开了一种洗碗机喷淋组件及洗碗机，属于厨具领域，洗碗机喷淋组件包括喷淋器本体、喷淋器套和滑轮；所述喷淋器本体转动的设置在洗碗机的内胆壁的底板上，所述喷淋器套分别套设在所述喷淋器的两端，且所述喷淋器套能够在所述喷淋器的端部伸缩移动；所述弹性元件设置在所述喷淋器本体上，且所述弹性元件与所述喷淋器套相连接，所述弹性元件对所述喷淋器套具有弹性拉力；所述滑轮转动地设置在所述喷淋器套的端部。本方案中，通过内胆侧壁和滑轮维持喷淋器伸缩旋转的控制方式，增加喷淋区域，减少喷淋死角，提高喷淋效果，进而提高客户的使用舒适度和满意度，提高产品的市场竞争力。 【EN】The invention discloses a dish washing machine spraying assembly and a dish washing machine, belonging to the field of kitchen ware, wherein the dish washing machine spraying assembly comprises a sprayer body, a sprayer sleeve and a pulley; the sprayer body is rotatably arranged on a bottom plate of the inner container wall of the dish washing machine, the sprayer sleeves are respectively sleeved at two ends of the sprayer, and the sprayer sleeves can move in a telescopic manner at the end parts of the sprayer; the elastic element is arranged on the sprayer body and connected with the sprayer sleeve, and the elastic element has elastic tension to the sprayer sleeve; the pulley is rotatably arranged at the end part of the sprayer sleeve. In this scheme, maintain the flexible rotatory control mode of spray thrower through inner bag lateral wall and pulley, increase and spray the region, reduce and spray the dead angle, improve and spray the effect, and then improve customer's use comfort and satisfaction, improve the market competition of product.

摘要：【中文】本发明公开了一种洗碗机喷淋组件及洗碗机，属于厨具领域，洗碗机喷淋组件包括喷淋器本体、喷淋器套和滑轮；所述喷淋器本体转动的设置在洗碗机的内胆壁的底板上，所述喷淋器套分别套设在所述喷淋器的两端，且所述喷淋器套能够在所述喷淋器的端部伸缩移动；所述滑轮转动地设置在所述喷淋器套的端部。本方案中，通过内胆侧壁和滑轮维持喷淋器伸缩旋转的控制方式，增加喷淋区域，减少喷淋死角，提高喷淋效果，进而提高客户的使用舒适度和满意度，提高产品的市场竞争力。 【EN】The invention discloses a dish washing machine spraying assembly and a dish washing machine, belonging to the field of kitchen ware, wherein the dish washing machine spraying assembly comprises a sprayer body, a sprayer sleeve and a pulley; the sprayer body is rotatably arranged on a bottom plate of the inner container wall of the dish washing machine, the sprayer sleeves are respectively sleeved at two ends of the sprayer, and the sprayer sleeves can move in a telescopic manner at the end parts of the sprayer; the pulley is rotatably arranged at the end part of the sprayer sleeve. In this scheme, maintain the flexible rotatory control mode of spray thrower through inner bag lateral wall and pulley, increase and spray the region, reduce and spray the dead angle, improve and spray the effect, and then improve customer's use comfort and satisfaction, improve the market competition of product.

摘要：【中文】本发明提供一种针对图像中矩形目标的高精度图像分割方法，涉及图像处理技术领域，所述方法包括步骤1：将图像读入内存，并对图像进行畸变矫正；步骤2：确定畸变矫正后图像矩形轮廓的四个端点，并对图像进行透视变换；步骤3：对透视变换后的图像进行分割，得到平直图像。本发明通过对矩形工件图像进行变换和分割处理，将工件图像中的矩形轮廓区域提取出来，并根据矩形工件图像的内部网格进行分割，保证分割位置正好处于矩阵工件图像的边界或者网格边界上，保证图像分割的准确度。 【EN】The invention provides a high-precision image segmentation method for a rectangular target in an image, which relates to the technical field of image processing, and comprises the following steps of 1: reading the image into a memory, and carrying out distortion correction on the image; step 2: determining four end points of the rectangular outline of the image after the distortion correction, and carrying out perspective transformation on the image; and step 3: and segmenting the image after perspective transformation to obtain a flat image. The rectangular outline area in the workpiece image is extracted by transforming and segmenting the rectangular workpiece image, and segmentation is carried out according to the internal grid of the rectangular workpiece image, so that the segmentation position is just positioned on the boundary of the matrix workpiece image or the grid boundary, and the accuracy of image segmentation is ensured.